ABSTRACTS
A. N. Arsenyev, M. Z. Muradymov, N. V. Krasnov |
FIELD DESORPTION OF IONS FROM THE TIP
TO THE MENISCUS OF THE LIQUID AT THE EHD-SPRAYING
|
Investigated modes of operation and current characteristics of the
device with a dynamic division electrospray flow sprayed liquid and removing the exess of the spray under normal
conditions. The existence of three most typical spray patterns: electrospray, field desorption, flow. Demonstrated
that the spray mode "field desorption" stability spraying currant and quantity not dependent on the flow
of sprayed liquid in the range 50–200 µl/min.
REFERENÑES
- Samokish V.A., Krasnov N.V., Muradymov M.Z. Electrospray ion sourse with a dynamic liquid flow splitter. Rapid Commun. Mass Spectrometry., 2013, no. 27 (8), pp. 904–908. DOI 10.1002/rcm 6524.
- Dole M., Mack L.L., Hines R.L. et al. Molecular beams of macroions. J. Chem. Physics. 1968, vol. 49, no. 5, pp. 2240–2249.
- Thermo Scientific. URL: (www.tectronica.com).
- Shimadzu Corp. URL: (www.Shimadzu.com).
- Agilent. URL: (www.Agilent.com).
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Institute for Analytical Instrumentation RAS, Saint-Petersburg, RF Contacts: Krasnov Nikolay Vasilyevich,
krasnov@alpha-ms.com
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p. 3-8 |
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V. V. Panchuk1,2, S. M. Irkaev1,
V. G. Semenov1,2 |
IMPROVEMENT OF DESIGN FOR RESONANCE DETECTION
IN MÖSSBAUER SPECTROSCOPY
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Improvement of design for resonance detection in Mössbauer
spectroscopy is proposed. Such improvement not limited with the choice of source-converter pairs and allows us
to choose various chemical compounds for resonant converter with a maximum content of resonant isotope. This
solution leads to an increase of the spectrum quality, its resolution and significantly reduces analysis time.
Experimentally demonstrated the influence of source-converter shift on the form of Mössbauer spectrum.
REFERENÑES
- Belyaev À.À., Irkaev S.M., Panchuck V.V. et al. American Institute of Physics Conference Proceedings, 2008, vol. 1070, pp. 147.
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1Institute for Analytical Instrumentation of RAS, Saint-Petersburg, RF
2Saint-Petersburg State University,
Contacts: Irkaev Sobir Mulloevich,
sobir_irkaev@mail.ru
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p. 9-15 |
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M. S. Gorbunov1, A. Yu. Portnoy2, G. V. Pavlinsky1 |
AN ESTIMATION OF GEOMETRY FACTOR INFLUENCE OF EDXRF SPECTRA TAKING INTO ACCOUNT MULTIPLE SCATTERING |
The current mathematical models of taking into account of influence of geometry
factor on signal to background ratio are considered in case of real EDXRF spectrometers. The model of multiple
scattering based on electron and photon radiation transport in elements of spectrometer using the Monte Carlo
method is proposed. It is shown that taking into account multiple scattering lead to better agreement between
experimental and calculated data.
REFERENÑES
- Fernandez J.E., Hubbell J.H., Hanson A.L., Spenser L.V. Polarization effects on multiple scattering gamma transport. Radiation Physics and Chemistry, 1993, vol. 41, no. 4/5, pp. 579–630.
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1Applied Physics Institute of Irkutsk State University, Irkutsk, RF
2Irkutsk State University of Transport, Irkutsk, RF Contacts: Gorbunov Michail, romepatrician@rambler.ru
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p. 16-21 |
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G. E. Rudnitskaya1, T. A. Lukashenko1, Y. S. Posmitnaya1,2,
A. N. Tupik1, A. A. Evstrapov1,2,3
|
PHYSICAL AND CHEMICAL METHODS FOR SURFACE
MODIFICATION OF POLY METHYL METHACRYLATE
MICROFLUIDIC CHIPS
|
One of the most common polymeric materials used to fabrication
the microfluidic chips is polymethylmethacrylate. Although the polymer has the desired physical and chemical
properties for many applications in analytical chemistry, medicine, biotechnology, but its hydrophobicity and
lack of reactive groups on the surface leads to a modification. The paper presents the results of studies of
chemical and physical processing methods to improve the surface wetting and create conditions for the subsequent
organization of functional groups.
REFERENÑES
- Alrifaiy A., Lindahl O.A., Ramser K. Polymer-based microfluidic devices for pharmacy, biology and tissue engineering. Polymers, 2012, vol. 4, pp. 1349–1398.
- Becker H., Gartner C. Polymer microfabrication technologies for microfluidic systems. Analytical and Bio-analytical Chemistry, 2008, vol. 390, no. 1. pp. 89–111.
- Lee S.-J. J., Sundararajan N. Microfabrication for microfluidics. MA, Norwood, ARTECH House Inc, 2010, 280 p.
- Ledesma-Aguilar R., Nistal R., Hernandez-Machado A., Pagonabarraga A. Controlled drop emission by wetting properties in driven liquid filaments. Nature Materials, 2011, vol. 10, pp. 367–371.
- Witters D., Vergauwe N., Vermeir S. et al. Biofunctio-nalization of electrowetting on dielectric digital micro-fluidic chips for miniaturized cell-based applications. Lab Chip, 2011, vol. 11, pp. 2790–2794.
- Wu D., Zhao B., Dai Z., Qin J., Lin B. Grafting epoxy-modified hydrophilic polymers onto poly (dimethylsi-loxane) microfluidic chip to resist nonspecificprotein adsorption. Lab Chip, 2006, vol. 6, pp. 942–947.
- Grainger D.W., Greef C.H., Gong P., Lochhead M.J. Current microarray surface chemistries. Methods in Molecular Biology, 2007, vol. 381, pp. 35–57.
- Carlborg C.F., van der Wijngaart W. Sustained super-hydrophobic friction reduction at high liquid pressures and large flows. Langmuir, 2011, vol. 27, pp. 487–493.
- Muck A., Svatos A. Chemical modification of polymeric microchip devices. Talanta, 2007, vol. 74, pp. 333–341.
- Stratakis E., Ranella A., Fotakis C. Biomimetic micro / nanostructured functional surfaces for microfluidic and tissue engineering applications. Biomicrofluidics, 2011, vol. 5, 013411, pp. 31.
- Kitova S., Minchev M., Danev G. Soft plasma treatment of polymer surfaces. Journal of Optoelectronics and Advanced Materials, 2005, vol. 7, no. 1, pp. 249–252.
- Brown L., Koerner T., Horton J.H., Oleschuk R.D. Fabrication and characterization of poly (methylmetha-crylate) microfluidic devices bonded using surface modifications and solvents. Lab Chip, 2006, vol. 6, pp. 66–73.
- Vesel A., Mozetic M. Surface modification and ageing of PMMA polymer by oxygen plasma treatment. Vacuum, 2012, vol. 86, no. 6, pp. 634–637.
- Chai J., Lu F., Li B., Kwok D. Y. Wettability Interpretation of Oxygen Plasma Modified Poly (methyl methacrylate). Langmuir, 2004, v. 20, no. 25, pp. 10919–10927.
- Mathur A., Roy S.S., Tweedie M. et al. Characterisation of PMMA microfluidic channels and devices fabricated by hot embossing and sealed by direct bonding. Curr. Appl. Phys., 2009, vol. 9, pp. 1199–1202.
- Jafari M., Dorranian D. Surface modification of PMMA polymer in the interaction with oxygen-argon RF plasma. Journal of Theoretical and Applied Physics, 2011, v. 5, no. 2, pp. 59–66.
- Tennico Y.H., Koesdjojo M.T., Kondo S. et al. Surface modification-assisted bonding of polymer-based microfluidic devices. Sensors and Actuators B, 2010, vol. 143, pp. 799–780.
- Cheng J.-Y., Wei C.-W., Hsu K.-H. Direct-write laser micromachining and universal surface modification of PMMA for device development. Sensors and Actuators B, 2004, vol. 99, no. 1, pp. 186–196.
- Mathur A., Roy S.S., Tweedie M. et al. Characterisation of PMMA microfluidic channels and devices fabricated by hot embossing and sealed by direct bonding. Curr. Applied Physics, 2009, vol. 9, no. 6, pp. 1199–1202.
- Yao L., Liu B., Chen T., Liu S., Zuo T. Micro flow-through PCR in a PMMA chip fabricated by KrF excimer laser. Biomed Microdevices, 2005, vol. 7, no. 3, pp. 253–257.
- Chen Y., Zhang L., Gang C. Fabrication, modification and application of Poly (methyl methacrylate) microfluidic chips. Electrophoresis, 2008, vol. 29, no. 9, pp. 1801–1814.
- Brown L., Koerner T., Horton J.H., Oleschuk R.D. Fabrication and characterization of poly (methylmetha-crylate) microfluidic devices bonded using surface modifications and solvents. Lab on Chip, 2006, vol. 6, no. 1, pp. 66–73.
- Israelachvili J.N., Gee M.L. Contact angles on chemically heterogeneous surfaces. Langmuir, 1989, vol. 5, no. 1, pp. 288–289.
- Peth C., Barkusky F., Mann K. Near-edge x-ray absorption fine structure measurements using a laboratory-scale XUV source. Journal of Physics D: Appl. Physics, 2008, vol. 41, no. 10, 105202.
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1Institute for Analytical Instrumentation of RAS, Saint-Petersburg
2University ITMO
3Saint-Petersburg Academic University — Nanotechnology Research and Education Center RAS
Contacts: Evstrapov Anatoly Alexandrovich, an_evs@mail.ru
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p. 22-31 |
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L. À. Obvintseva1, Ò. B. Tsyrkina1,
I. P. Sukhareva1, I. B. Belikov2, À. Ê. Avetisov1 |
RESPONSE FEATURES OF THE GAS SENSOR
RESISTIVE IN FLOW MODE
|
Presented are experimental results of investigation of gas
flow velocity influence on the sensitive layer resistance of the resistive semiconductor sensor under
condition of heater thermo stabilization and sensor design when heater and sensitive layer are on the
opposite sides of the dielectric substrate. It is shown, that change in sensor sensitive layer resistance
caused by flow velocity changes under condition of constant heater temperature repeats the character of
temperature dependence of sensor sensitive layer resistance in a constant flow. Influence of the observed
dependences for the results of the ozone concentration measurements is discussed.
REFERENÑES
- Korotchenko G., Cho B.K. Instability of metal oxide-based conductometric gas sensors and approaches to stability improvement (short survey). Sensors and Actuators B, 2011, vol. 156, pp. 527–538.
- Giberti A., Benetti M, Carotta M.C. et al. Heat exchange and temperature calculation in thick-film semiconductor gas sensor systems. Sensors and Actuators B, 2008, vol. 130, pp. 277–280.
- Isaienko O., Maksymovych N., Yatsimirsky V. Determination of the sensitive layer temperature of the adsorption-semiconductor gas sensor. Sensors and Actuators B, 2005, vol. 108, pp. 134–142.
- Calestani D., Zha M., Mosca R. et al. Growth of ZnO tetrapods for nanostructure-based gas sensors. Sensors and Actuators B, 2010, vol. 144, no. 2, pp. 472–478.
- Korotcenkov G., Cho B.K. Ozone measuring: What can limit application of SnO2-based conductometric gas sensors? Sensors and Actuators B, 2012, vol. 161, pp. 28–44.
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1Karpov Institute of Physical Chemistry, Moscow, RF
2Obukhov Institute of Atmospheric Physics, Russian Academy of Sciences, Moscow, RF
Contacts: Obvintseva Ludmila Alexeevna, obvint@yandex.ru
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p. 32-41 |
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D. V. Dvorzov, V. A. Parfenov |
SPECTRAL CHARACTERISTICS OF SINGLE-FREQUENCY
MODE OF OPERATION OF DIODE LASERS
|
The researches, which have been carried by authors, are concerned
with study of single-frequency mode of operation of diode lasers generating at the wavelengths of 635 and 655 nm.
In our experiments we have studied spectral characteristics of these lasers (presence of single-longitudinal-mode, inter-mode interval,
range of temperature tuning of frequency of laser radiation, measurements of drift of average value of frequency in time).
REFERENÑES
- ThorLabs. URL: (http://www.thorlabs.de/newgrouppage9.cfm?objectgroup_id=7).
- Wieman C.E., Hollberg L. Using diode lasers for atomic physics. Rev. Sci. Instr., 1991, vol. 62, no. 1, pp. 1–20.
- Fox R.W., Hollberg L., Zibrov A.S. Semiconductor diode laser. Atomic, Molecular, and Optical Physics: Electromagnetic Radiation, Academic Press, San Diego, 1997, vol. 29C, Eds. Dunning F.B. and Hulet R.G. pp. 77–102.
- DL-100 Series — Tunable Diode Lasers. URL: (http://www.toptica.com/products/research_grade_diode_lasers/tunable_diode_lasers/tunable_diode_lasers_370_nm_1770_nm_dl_100.html).
- URL: (http://www.nevatec.ru/LR/index.htm).
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Saint-Petersburg Polytechnic University, RF
Contacts: Parfenov Vladimir Alexandrovich,
ppparfen@mail.ru;
Dvorzov Denic Valerievich,
otenki@mail.ru
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p. 42-48 |
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A. S. Polyakov1, N. V. Konenkov1, A. S. Berdnikov2 |
MASS PEAK SHAPE OF THE LINEAR ION TRAP
WITH CYLINDRICAL RODS AT QUADRUPOLAR RESONANCE
EXCITATION OF THE CONFINED IONS
|
Linear ion trap excitation contour with round rods is studied by the
numerical method in dependence of geometrical parameter γ = r / r0, where r is the rod
radius, r0 is a radius of the inscribed circular between rod tips. The quadrupole resonance parametric
excitation of the ion oscillations by three methods: (a) auxiliary RF voltage, (b) amplitude and (c) frequency (phase)
modulation of the applied RF voltage have been studied. It was obtained that irrespective of the above methods the
peak shape is symmetrical and has a slow peak tails for ratio r / r0 = 1.12–1.13 thus the
resolution determined at half peak height is the same as for pure quadrupole field.
REFERENÑES
- Dawson P.H. Quadrupole mass spectrometry and its applications. Ed.: P.H. Dawson. Woodbury, AIP Press, 1995, 129 p.
- Dayton I.E., Shoemaker F.C., Mozley R.F. The measurement of two-dimensional fields. Part II: Study of a quadrupole magnet. Rev. Sci. Instr., 1952, vol. 25, p. 485–490.
- Denison D.R. Operating parameters of a quadrupole in a grounded cylindrical housing. J. Vac. Sci. Technol., 1971, vol. 8, p. 266–269.
- Lee-Whiting G.E., Yamazaki L. Semianalytical calculations for circular quadrupoles. Nucl. Instrum. Methods, 1971, vol. 94, p. 319–324.
- Reuben A.J., Radchik A.V., Smith G.B., Vagov A.V. Exact fields in multi-electrode ion optics. Rapid Commun. Mass Spectrom., 1994, vol. 8, p. 939–941.
- Reuben A.J., Smith G.B., Moses P. et al. Ion trajectories in exactly determined quadrupole fields. Int. J. Mass Spectrom. Ion. Proc., 1996, vol. 153, p. 43–59.
- Schulte J., Shevchenko P.V., Radchik A.V. Nonlinear field effects in quadrupole mass filters. Rev. Sci. In-strum., 1999, vol. 70, no. 9, p. 3566–3571.
- Gibson J.R., Taylor S. Numerical investigation of the effect of electrode size on the behavior of quadrupole mass filters. Rapid Commun. Mass Spectrom., 2001, vol. 15, p. 1960–1964.
- Douglas D.J., Konenkov N.V. Influence of the 6th and 10th spatial harmonics on the peak shape of a quadrupole mass filter with round rods. Rapid Commun. Mass Spectrom., 2002, vol. 16, p. 1425–1431.
- Douglas D.J., Konenkov N.V. Mass resolution of linear quadrupole ion traps with round rods. Rapid Commun. Mass Spectrom., 2014, in press.
- Konenkov N.V., Cousins L.M., Baranov V.I. et al. Quadrupole mass filter operation with auxiliary quadrupole excitation: Theory and experiment. Int. J. Mass Spectrom., 2001, vol. 208, p. 17–27.
- Konenkov N.V., Douglas D.J., Sudakov M.Yu. Matrix methods for the calculation of the stability diagrams in quadrupole mass spectrometry. J. Am. Soc. Mass Spectrom., 2002, vol. 13, no. 6, p. 597–613.
- Konenkov N.V., Korolkov A.N., Makhmudov M.N. Upper stability island of the quadrupole mass filter with amplitude modulation of the applied voltages. J. Am. Soc. Mass Spectrom., 2005, vol. 16, p. 379–387.
- Luo C., Jiang D., Ding C.-F., Konenkov N.V. Mass peak shape improvement of a quadrupole mass filter when operating with a rectangular wave power supply. Rapid Commun. Mass Spectrom., 2009, vol. 23, no. 17, p. 2793–2801.
- Zhao X., Ryjkov V.L., Schuessler H.A. Parametric excitations of trapped ions in a linear rf ion trap. Physical Review A, 2002, vol. 66, 063414, p. 1–7.
- Gershman D.J., Block B.P., Rubin M. et al. Higher order parametric excitation modes for spaceborne quadrupole mass spectrometers. Rev. Sci. Instrum., 2011, 125109, p. 1–15.
- Konenkov A.N., Douglas D.J., Konenkov N.V. Spatial harmonics of linear multipoles with round electrodes. Int. J. Mass Spectrom., 2010, vol. 289, p. 144–149.
- Douglas D.J., Konenkov N.V. Mass selectivity of dipolar resonant excitation in a linear quadrupole ion trap. Rapid Commun. Mass Spectrom., 2014, vol. 28, p. 430–439.
- Douglas D.J., Polyakov A. and Konenkov N.V. Quadrupolar ion excitation for radiofrequency-only mass filter operation. Eur. J. Mass Spectrom., 2014, vol. 20, p. 207–214.
- Konenkov N.V., Londry F., Ding C.-F., Douglas D.J. Linear quadrupoles with added hexapole fields. J. Am. Soc. Mass Spectrom., 2005, vol. 17, p. 1063–1073.
- Ding C.-F., Konenkov N.V., Douglas D.J. Quadrupole mass filters with octopole fields. Rapid Commun. Mass Spectrom., 2003, vol. 17, p. 2495–2502.
- Prog. Mathematica. URL: (http://www.wolfram.com).
- Prog. Simion. URL: (http://www.simion.com).
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1Ryazan State University, Ryazan, RF
2Institute for Analytical Instrumentation of RAS, Saint-Petersburg, RF
Contacts: Konenkov Nikolay Vital'evich, n.konenkov@rsu.edu.ru
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p. 49-61 |
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A. S. Berdnikov1, N. R. Gall1,2,3 |
SPECIFICS OF NUMERICAL SIMULATIONS OF THE TRAJECTORIES OF
CHARGED PARTICLES IN PULSED ELECTRIC FIELDS |
The problem of numerical simulation of the trajectories of charged
particles as applied to the pulsed electric fields, is considered. Typical numerical recipes imply that the right
hand side function of the differential equations is smooth and can be differentiated up to necessary order; however,
when applied to the functions with sharp jumps these recipes can result to serious inaccuracies of the calculations.
The paper considers the true inaccuracy artifacts which exists for the pulsed functions (pulsed electric fields) when
some "smooth" numerical recipes are used for trajectory integration. It also considers some simple
modifications of the standard tracing algorithms which enable to eliminate these artifact effects.
REFERENÑES
- Hawkes P.W., Kasper E. Principles of electron optics. London, 1989.
- Yavor M.I. Optics of charged particle analyzers. Ser. Advances of Imaging and Electron Physics, Amsterdam, Elsevier, 2009, vol. 157.
- Kutta M.W. Beitrag zur näherungsweisen integration totaler differentialgleichungen. Zeitschrift für Mathematik und Physik, 1901, vol. 46, ðp. 435–453.
- Press W.H., Teukolsky S.A., Vetterling W.T., Flannery B.P. Numerical recipes: the art of scientific computing. Third edition. Cambridge University Press, 2007, 1235 ð. URL: (http://www.nr.com).
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1Institute for Analytical Instrumentation of RAS, Saint-Petersburg
2A.F. Ioffe Physico-Technical Institute of RAS, Saint-Petersburg
3Saint-Petersburg State Polytechnical University
Contacts: Berdnikov Alexander Sergeevich, asberd@yandex.ru
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p. 62-74 |
|
B. P. Sharfarets |
APPROXIMATE METHOD OF THE SOLUTION OF TASKS
MULTIPLE DISPERSION IN THE HALF-SPACE
|
Questions of the approximate accounting of multiple dispersion in
the conditions of influence of borders of a wave guide are considered. The problem is solved in relation to the
spherical radiator which is in a half-space at flat border. Expressions for direct, and also the field once
disseminated by a radiator caused by existence of waves reflected from border are presented. The problem is
solved in zero approach by means of received before the equipment following from that fact that amplitude of
dispersion satisfies to Helmholtz's equation on variables of location of the lens.
REFERENÑES
- Gaunaurd J.C., Huang H. Acoustic scattering by a spherical body a plane boundary. J. Acoust. Soc. Am., 1994, vol. 96, no. 4, pp. 2526–2536.
- Gaunaurd J.C., Huang H., Strifors H.C. Acoustic scattering by a pair of spheres. J. Acoust. Soc. Am., 1995, vol. 96, no. 1, pp. 495–507.
- Colton D., Kress R. Inverse acoustic and electromagnetic scattering theory. Springer, 1998. 334 p.
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Institute for Analytical Instrumentation of RAS, Saint-Petersburg, RF
Contacts: Sharfarets Boris Pinkusovich, sharb@mail.ru
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p. 75-79 |
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B. P. Sharfarets |
TO THE QUESTION OF THE APPROXIMATE METHOD
OF THE DECISION PROBLEMS OF MULTIPLE DISPERSION.
THE DECISION ON THE EXAMPLE OF THE IDEAL WAVE GUIDE
|
In work on the example of the elementary liquid layer with flat
borders the general rather simple approximate algorithm of calculation of the field formed by dispersion of primary
field radiated by a third-party source on inclusion and dispersion on inclusion of a secondary field after its single
reflection from borders of a wave guide is offered. The secondary field is understood as the field of dispersion
caused by falling on inclusion of primary field. The task is considered for inclusion in the form of any spherically
a symmetric body, however this assumption is easily generalized on any inclusion. The solution of this task was
possible thanks to the algorithm of stay of total amplitude of dispersion received earlier by the author when falling
on inclusion of a wave of a difficult form. The algorithm can be used in layered and non-uniform wave guides on
condition of uniformity of the layer containing inclusion. The problem is easily solved and when the radiator and
inclusion are combined.
REFERENÑES
- Hackman R.H., Sammelmann G.S. Acoustic scattering in an inhomogeneous waveguide: Theory. J. Acoust. Soc. Am., 1986, vol. 80, no. 5, pp. 1447–1458.
- Sammelmann G.S., Hackman R.H. Acoustic scattering in a homogeneous waveguide: Theory. J. Acoust. Soc. Am., 1987, vol. 82, no. 1, pp. 324–336.
- Hackman R.H., Sammelmann G.S. Multiple-scattering analysis for a target in an oceanic waveguide. J. Acoust. Soc. Am., 1988, vol. 84, no. 5, pp. 1813–1825.
- Gaunaurd J.C., Huang H. Acoustic scattering by a Spherical body a plane boundary. J. Acoust. Soc. Am., 1994, vol. 96, no. 4, pp. 2526–2536.
- Gaunaurd J.C., Huang H., Strifors H.C. Acoustic scat-tering by a pair of spheres. J. Acoust. Soc. Am., 1995, vol. 96, no. 1, pp. 495–507.
- Colton D., Kress R. Inverse acoustic and electromag-netic scattering theory. Springer, 1998, 334 p.
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Institute for Analytical Instrumentation of RAS, Saint-Petersburg, RF
Contacts: Sharfarets Boris Pinkusovich, sharb@mail.ru
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p. 80-86 |
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D. A. Belov, Yu. V. Belov, V. V. Manoylov, V. E. Kurochkin |
METHODS OF GENETIC ANALYSIS RESULTS PROCESSING
|
The genetic signals simulation for assessment of digital signal
processing efficiency was carried out. The possibilities of different methods of baseline correction, filtering
and increasing resolution in genetic analyses were considered.
REFERENÑES
- URL: (http://www.iai.rssi.ru/en/catalog.php).
- URL: (http://matlab.exponenta.ru/ml/book2/chapter8/diff.php).
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Institute for Analytical Instrumentation of RAS, Saint-Petersburg, RF
Contacts: Manoylov Vladimir Vladimirovich, manoilov_vv@mail.ru;
Belov Yuriy Vasil'evich, bel3838@mail.ru
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p. 87-91 |
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A. V. Borodin1, V. A. Borodin2, K. N. Smirnov2, D. B. Shiryaev2,
D. N. Frantzev1, M. V. Yudin1
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APPARATUS FOR GROWING SAPPHIRE SINGLE CRYSTALS
BY KYROPOULOS METHOD WITH DYNAMIC WEIGHING DEVICE AND AUTOMATIC FEEDBACK CONTROL
|
Currently Kyropoulos method (GOI) is the most widely applied for
industrial production of single sapphire crystals of optoelectronic quality. The method consists in the fact that
growth of the crystal is carried out directly in the melt by gradual temperature decrease. Generally, process control
is based on reducing the heating power according to a predetermined function of time which is chosen empirically on
the grounds of quality of crystals obtained in preceding processes. In recent years, weight sensors have been used
to control the process of crystal growing by Kyropoulos method. The main advantage of the crystallization process
control using dynamic weighing is the ability to measure continuously and stabilize the crystallization mass rate
using a feedback system. However, implementation this system requires the development of high-precision dynamic
weighing apparatus, as well as algorithms for automatic feedback control. In this paper we consider the design
features and algorithms for automatic control applied for NIKA-M60 crystal growth machine. These features allow
realizing automatic control crystallization process with feedback via the heater power and the pulling rate of
the crystal.
REFERENÑES
- URL: (http://www.apeks-sapphire.com/Rus/equipment_ru.html).
- Bardsley W., Green G.W., Holliday C.H., Hurle D.T.J. Automatic control of Czochralski crystal growth. J. of Crystal Growth, 1972, vol. 16, pp. 277–279.
- URL: (http://www.rsatu.ru/arch/aref_lobacevich_kl.pdf).
- Singh G., Ghosh B., Deshpande R.Y. On the shape of crystals grown by Kyropoulos technique. Kristall und Technik, 1981, vol. 16, pp. 1239–1245.
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1Federal State Institution of Science Institute of Solid State Physics, RAS (ISSP), Chernogolovka, RF
2The Federal State Unitary Enterprise Experimental Factory of Scientific Engineering with the Special Design Bureau of the RAS (EZAN), Chernogolovka, RF
Contacts: Francev Dmitry Nikolaevich, far-far@mail.ru
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p. 92-98 |
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A. V. Borodin1, V. A. Borodin2, D. N. Frantzev1, M. V. Yudin1, T. A. Mosharov2 |
TECHNOLOGY AND AUTOMATED EQUIPMENT
FOR THE PRODUCTION OF PROTECTIVE SAPPHIRE SCREENS FOR PORTABLE MOBILE DEVICES (short message)
|
Currently, the major manufacturers of mobile communication devices
(smartphones, tablets) started to use sapphire as a protective material for a screen. Strength and high hardness
of sapphire significantly improve consumer quality of smartphones, and is just necessary for devices required for
a special purpose. The mass use and substitution of traditional chemically toughened glass with sapphire so far
limited due to its high cost of production and mechanical processing. Ezan develops and delivers high-performance
industrial equipment and technology for production of shaped sapphire crystals. The equipment and technology has
advantages it terms of cost and productivity over the well-established techniques used for commercial production
of protective screens for mobile devises
REFERENÑES
- URL: (http://lugansk.all.biz/oborudovanie-dlya-vyrashchivaniya-profilnyh-g1551388#.U8URa_l_t8E).
- URL: (http://omega-crystals.com/ru/product/Spektr_DM-4.html).
- A durable and scratch-free screen cover material for next-generation mobile and touch screen devices. URL: (www.gtat.com/7a480e6e-3b40.../download.htm).
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1Federal State Institution of Science Institute of Solid
State Physics, RAS (ISSP), Chernogolovka, RF
2The Federal State Unitary Enterprise Experimental Factory of Scientific Engineering with the Special Design Bureau of the RAS (EZAN), Chernogolovka, RF
Contacts: Yudin Mikhail Viktorovich, mikhail-yu@inbox.ru
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p. 99-104 |
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